3-nitro-4-chlorobenzenediazonium cation

Base Information

• Chemical Name: 3-nitro-4-chlorobenzenediazonium cation
• CAS No.: 30930-62-2
• Molecular Formula: C₆H₃ClN₃O₂
• Molecular Weight: 184.562
• Mol file: 30930-62-2.mol

Synonyms:3-nitro-4-chlorobenzenediazonium cation

Chemical Property of 3-nitro-4-chlorobenzenediazonium cation

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-nitro-4-chlorobenzenediazonium cation

There total 1 articles about 3-nitro-4-chlorobenzenediazonium cation which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + 3,4-dinitroaniline (610-41-3) + acetic acid (64-19-7,77671-22-8) → 3-nitro-4-chlorobenzenediazonium cation (30930-62-2)

Guidance literature:

at 40 ℃; Geschwindigkeit;

Reference yield:

3-nitro-4-chlorobenzenediazonium cation (30930-62-2) + sodium methylate (124-41-4) → 2-Nitroanisole (91-23-6) + 2-Chloronitrobenzene (88-73-3) + 2-chloro-5-methoxynitrobenzene (10298-80-3)

Guidance literature:

for 16h; Mechanism; Ambient temperature; also reaction with sodium deuteriomethoxide;

DOI:10.1071/CH9831031

Reference yield:

3-nitro-4-chlorobenzenediazonium cation (30930-62-2) → 3-nitro-4-chlorobenzenediazohydroxide (51090-29-0)

Guidance literature:

With hydroxide; at 19.9 ℃; Equilibrium constant;

upstream raw materials:

hydrogenchloride

3,4-dinitroaniline

acetic acid

Downstream raw materials:

2-Nitroanisole

2-Chloronitrobenzene

2-chloro-5-methoxynitrobenzene

3-nitro-4-chlorobenzenediazohydroxide