pyridine-benzylcyanoborate

Base Information

Chemical Name:pyridine-benzylcyanoborate
CAS No.:124287-41-8
Molecular Formula:C₅H₅N*C₈H₈BN
Molecular Weight:208.071
Hs Code.:

Synonyms:pyridine-benzylcyanoborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pyridine-benzylcyanoborate

Chemical Property:

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Technology Process of pyridine-benzylcyanoborate

There total 4 articles about pyridine-benzylcyanoborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 628-13-7
pyridine hydrochloride

: 592-04-1
mercury(II) cyanide

: 162213-35-6
C₁₃H₂₁BO₂

: 124287-41-8
pyridine-benzylcyanoborate

Guidance literature:: C₁₃H₂₁BO₂; With lithium aluminium tetrahydride; In diethyl ether;

mercury(II) cyanide; In tetrahydrofuran; Heating;

pyridine hydrochloride; In tetrahydrofuran; Heating;
DOI:10.1039/b006265k

Reference yield:

: 108-88-3,15644-74-3,16713-13-6
toluene

: 124287-41-8
pyridine-benzylcyanoborate

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi; TMEDA / Heating

1.2: -78 - 20 °C

1.3: 85 percent / AcCl

2.1: LiAlH₄ / diethyl ether

2.2: tetrahydrofuran / Heating

2.3: 69 percent / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether;
DOI:10.1039/b006265k

Reference yield:

: 110-86-1
pyridine

: 124287-32-7
trimethylamine-benzylcyanoborane

: 124287-41-8
pyridine-benzylcyanoborane

Guidance literature:: In pyridine; trimethylamine-benzylcyanoborane dissolved in pyridine at room temp. or at 70°C; reaction monitored by chiral HPLC;
DOI:10.1039/b006265k