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C30H47N3O7Si2

Base Information
  • Chemical Name:C30H47N3O7Si2
  • CAS No.:1311295-67-6
  • Molecular Formula:C30H47N3O7Si2
  • Molecular Weight:617.89
  • Hs Code.:
C<sub>30</sub>H<sub>47</sub>N<sub>3</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C30H47N3O7Si2

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Chemical Property of C30H47N3O7Si2
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Technology Process of C30H47N3O7Si2

There total 11 articles about C30H47N3O7Si2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With palladium diacetate; silver carbonate; In tert-butyl alcohol; at 70 ℃; for 40h; regioselective reaction; Darkness;
DOI:10.1002/anie.201100984
Guidance literature:
Multi-step reaction with 5 steps
1.1: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C
1.2: 2 h / 20 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
3.1: palladium on carbon; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr
4.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 30 h / 80 °C / Darkness
5.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 40 h / 70 °C / Darkness
With 1H-imidazole; palladium on carbon; hydrogen; palladium diacetate; silver carbonate; sodium hydroxide; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/anie.201100984
Guidance literature:
Multi-step reaction with 7 steps
1.1: 2 h / Reflux
2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 0 - 20 °C
2.2: 2 h / 20 °C
3.1: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C
3.2: 2 h / 20 °C
4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
5.1: palladium on carbon; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr
6.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 30 h / 80 °C / Darkness
7.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 40 h / 70 °C / Darkness
With 1H-imidazole; palladium on carbon; hydrogen; palladium diacetate; 1,1'-carbonyldiimidazole; silver carbonate; sodium hydroxide; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/anie.201100984
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