Technology Process of C30H47N3O7Si2
There total 11 articles about C30H47N3O7Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; silver carbonate;
In
tert-butyl alcohol;
at 70 ℃;
for 40h;
regioselective reaction;
Darkness;
DOI:10.1002/anie.201100984
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C
1.2: 2 h / 20 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
3.1: palladium on carbon; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr
4.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 30 h / 80 °C / Darkness
5.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 40 h / 70 °C / Darkness
With
1H-imidazole; palladium on carbon; hydrogen; palladium diacetate; silver carbonate; sodium hydroxide;
In
tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/anie.201100984
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 2 h / Reflux
2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 0 - 20 °C
2.2: 2 h / 20 °C
3.1: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C
3.2: 2 h / 20 °C
4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
5.1: palladium on carbon; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr
6.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 30 h / 80 °C / Darkness
7.1: palladium diacetate; silver carbonate / tert-butyl alcohol / 40 h / 70 °C / Darkness
With
1H-imidazole; palladium on carbon; hydrogen; palladium diacetate; 1,1'-carbonyldiimidazole; silver carbonate; sodium hydroxide;
In
tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/anie.201100984