3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide

Base Information

Chemical Name:3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide
CAS No.:1207315-88-5
Molecular Formula:C₁₈H₇BrF₁₁N₃O
Molecular Weight:570.16
Hs Code.:

Synonyms:3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide

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Chemical Property of 3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide

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Technology Process of 3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide

There total 7 articles about 3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1207315-89-6
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

: 1207315-88-5
3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide

Guidance literature:: With ammonium carbonate; In dimethyl sulfoxide; at 100 ℃; for 5h;

Reference yield:

: 88-17-5
2-(trifluoromethyl)benzenamine

: 1207315-88-5
3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium dithionite / ethyl acetate; water / 6 h / 20 °C

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 60 °C

3: 1,3-dimethyl-2-imidazolidinone / 5 h / 130 °C

4: ammonium carbonate / dimethyl sulfoxide / 5 h / 100 °C

With 1,3-dimethyl-2-imidazolidinone; N-Bromosuccinimide; sodium dithionite; tetra(n-butyl)ammonium hydrogensulfate; ammonium carbonate; sodium hydrogencarbonate; In water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1033997-04-4
4-cyano-2,3-difluoro-benzoic acid

: 1207315-88-5
3-amino-N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2-fluorobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2: 1,3-dimethyl-2-imidazolidinone / 5 h / 130 °C

3: ammonium carbonate / dimethyl sulfoxide / 5 h / 100 °C

With 1,3-dimethyl-2-imidazolidinone; oxalyl dichloride; ammonium carbonate; N,N-dimethyl-formamide; In dichloromethane; dimethyl sulfoxide;