N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

Base Information

Chemical Name:N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide
CAS No.:1207315-89-6
Molecular Formula:C₁₈H₅BrF₁₂N₂O
Molecular Weight:573.135
Hs Code.:

Synonyms:N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

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Chemical Property of N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

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Technology Process of N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

There total 4 articles about N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207315-90-9
4-cyano-2,3-difluorobenzoyl chloride

: 1207314-86-0
2-bromo-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-6-(trifluoromethyl)aniline

: 1207315-89-6
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

Guidance literature:: With 1,3-dimethyl-2-imidazolidinone; at 130 ℃; for 5h;

Reference yield:

: 88-17-5
2-(trifluoromethyl)benzenamine

: 1207315-89-6
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium dithionite / ethyl acetate; water / 6 h / 20 °C

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 60 °C

3: 1,3-dimethyl-2-imidazolidinone / 5 h / 130 °C

With 1,3-dimethyl-2-imidazolidinone; N-Bromosuccinimide; sodium dithionite; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1033997-04-4
4-cyano-2,3-difluoro-benzoic acid

: 1207315-89-6
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-cyano-2,3-difluorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2: 1,3-dimethyl-2-imidazolidinone / 5 h / 130 °C

With oxalyl dichloride; N,N-dimethyl-formamide; In 1,3-dimethyl-2-imidazolidinone; dichloromethane;