(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate

Base Information

Chemical Name:(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate
CAS No.:1426302-58-0
Molecular Formula:C₂₅H₃₅N₃O₆
Molecular Weight:473.569
Hs Code.:

Synonyms:(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate

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Chemical Property of (S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate

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Technology Process of (S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate

There total 8 articles about (S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426302-57-9
((S)-methyl 3-(tert-Butoxycarbonyl)amino)-4-(4-(3-oxopropoxy)phenyl)butanoate

: 10201-73-7
2-amino-4-methoxypyridine

: 1426302-58-0
(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate

Guidance literature:: With magnesium sulfate monohydrate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/anie.201206370

Reference yield:

: 1426302-56-8
(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-hydroxypropoxy)phenyl)butanoate

: 1426302-58-0
(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 6 h / 20 °C

2: magnesium sulfate monohydrate / dichloromethane / 1 h / 20 °C

With magnesium sulfate monohydrate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/anie.201206370

Reference yield:

: 949459-68-1
N-tert-butyloxycarbonyl-β-homotyrosine methyl ester

: 1426302-58-0
(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-((4-methoxypyridin-2-yl)amino)propoxy)phenyl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 6 h / 20 °C

3.1: magnesium sulfate monohydrate / dichloromethane / 1 h / 20 °C

With magnesium sulfate monohydrate; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/anie.201206370