(3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione

Base Information

• Chemical Name: (3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione
• CAS No.: 112878-92-9
• Molecular Formula: C₁₈H₁₆N₂O₂S
• Molecular Weight: 324.403

Synonyms:(3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione

Chemical Property of (3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

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Technology Process of (3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione

There total 6 articles about (3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.8%

C10H11NO2S + benzyl isothiocyanate (3173-56-6) → (3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione (112878-92-9)

Guidance literature:

In toluene; at 0 - 20 ℃; for 5h; Time; Reflux;

Reference yield: 90.0%

(4R)-2-phenyl-1,3-thiazolidine-4-carboxylic acid (196930-46-8) + benzyl isothiocyanate (3173-56-6) → (3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione (112878-92-9)

Guidance literature:

(4R)-2-phenyl-1,3-thiazolidine-4-carboxylic acid; benzyl isothiocyanate; In tetrahydrofuran; at 60 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; at 60 ℃; for 1.5h;

DOI:10.1016/j.tet.2005.07.070

Reference yield: 84.0%

(R)-3-Benzyl-5-mercaptomethyl-imidazolidine-2,4-dione (116615-89-5) + benzaldehyde (100-52-7) → (3S,7aR)-6-benzyl-3-phenyldihydro-3H,5H-imidazo[1,5-c]thiazole-5,7(6H)-dione (112878-92-9)

Guidance literature:

With toluene; trichlorophosphate; at 100 ℃; for 4h;

upstream raw materials:

(4R)-2-phenyl-1,3-thiazolidine-4-carboxylic acid

benzyl isothiocyanate

benzaldehyde

(R)-3-Benzyl-5-mercaptomethyl-imidazolidine-2,4-dione

Downstream raw materials:

(3S,7aR)-6-benzyl-7-hydroxy-3-phenyltetrahydro-5H-imidazo[1,5-c][1,3]thiazol-5-one

(3S,7aR)-6-benzyl-7-methoxy-3-phenyltetrahydro-5H-imidazo[1,5-c][1,3]thiazol-5-one

(3aS,4S,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-1H-thieno[3,4-d]imidazol-5-ylidene)pentanoic acid

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