Se-Butyl benzeneselenoate

Base Information

• Chemical Name: Se-Butyl benzeneselenoate
• CAS No.: 77129-68-1
• Molecular Formula: C₁₁H₁₄OSe
• Molecular Weight: 241.192
• Mol file: 77129-68-1.mol

Synonyms:Se-Butyl benzeneselenoate

Chemical Property of Se-Butyl benzeneselenoate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Se-Butyl benzeneselenoate

There total 6 articles about Se-Butyl benzeneselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

dibutyl diselenide (20333-40-8) + benzoic acid anhydride (93-97-0) → Se-Butyl benzeneselenoate (77129-68-1)

Guidance literature:

With magnesium; iron(II) chloride; In 1,4-dioxane; at 100 ℃; for 12h; Air;

DOI:10.1055/s-0029-1219229

Reference yield: 75.0%

dibutyl diselenide (20333-40-8) + benzoyl chloride (98-88-4) → Se-Butyl benzeneselenoate (77129-68-1)

Guidance literature:

With magnesium; iron(II) chloride; In 1,4-dioxane; at 100 ℃; for 12h; Air;

DOI:10.1055/s-0029-1219229

Reference yield:

α-bromoacetophenone (70-11-1) → Se-Butyl benzeneselenoate (77129-68-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / ethanol / 20 °C / Inert atmosphere

2: iron(III) chloride; dibenzoyl peroxide / dichloromethane / 3 h / 20 °C

With iron(III) chloride; sodium hydrogencarbonate; dibenzoyl peroxide; In ethanol; dichloromethane;

DOI:10.1016/j.tet.2019.130624

upstream raw materials:

1-bromo-butane

benzoyl chloride

n-butyllithium

dibutyl diselenide