8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine

Base Information

Chemical Name:8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine
CAS No.:116438-00-7
Molecular Formula:C₂₂H₂₂N₂O₄
Molecular Weight:378.428
Hs Code.:

Synonyms:8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine

Suppliers and Price of 8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine

There total 2 articles about 8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 546-67-8
lead(IV) tetraacetate

: 116437-99-1
8-amino-1-benzyl-6,9-dimethyl-2,5-dioxo-1,2,3,4,5,6-hexahydro-1-benzazocine

: 116438-00-7
8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine

Guidance literature:: In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1021/jo00257a031

Reference yield:

: 88609-66-9
1-Benzyl-8-(benzylamino)-6,9-dimethyl-2,5-dioxo-1,2,3,4,5,6-hexahydro-1-benzazocine

: 116438-00-7
8-(acetylimino)-1-benzyl-6,9-dimethyl-2,5,7-trioxo-1,2,3,4,5,6,7,8-1-benzazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂, / 20percent Pd(OH)2/C / ethyl acetate / 24 h / 760 Torr

2: 40 percent / CH₂Cl₂ / 0.25 h / 0 °C

With hydrogen; palladium dihydroxide; In dichloromethane; ethyl acetate;
DOI:10.1021/jo00257a031