1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene

Base Information

Chemical Name:1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene
CAS No.:158720-13-9
Molecular Formula:C₂₀H₃₆O₃Si
Molecular Weight:352.59
Hs Code.:

Synonyms:1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene

Chemical Property:

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Technology Process of 1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene

There total 5 articles about 1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 87541-83-1
1,4-dimethoxy-2-(3-hydroxypropyl)-3,5,6-trimethylbenzene

: 158720-13-9
1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene

Guidance literature:: With 1H-imidazole; dmap; In N,N-dimethyl-formamide; Ambient temperature;

Reference yield:

: 700-13-0
Trimethylhydroquinone

: 158720-13-9
1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / K₂CO₃ / acetone

2: 99 percent / Br₂, Fe / CH₂Cl₂ / 2 h / Ambient temperature

4: 1.) 1M (BH₃)2, 2.) 30percent H₂O₂, dil. NaOH / 1.) Et₂O, THF, 0 deg C, overnight, 2.) Et₂O, THF

5: 96 percent / imidazole, 4-(dimethylamino)pyridine / dimethylformamide / Ambient temperature

With 1H-imidazole; dmap; sodium hydroxide; diborane; dihydrogen peroxide; bromine; iron; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 4537-09-1
1,4-dimethoxy-2,3,5-trimethyl-benzene

: 158720-13-9
1-<3-(tert-butyldimethylsilyloxy)propyl>-2,5-dimethoxy-3,4,6-trimethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / Br₂, Fe / CH₂Cl₂ / 2 h / Ambient temperature

3: 1.) 1M (BH₃)2, 2.) 30percent H₂O₂, dil. NaOH / 1.) Et₂O, THF, 0 deg C, overnight, 2.) Et₂O, THF

4: 96 percent / imidazole, 4-(dimethylamino)pyridine / dimethylformamide / Ambient temperature

With 1H-imidazole; dmap; sodium hydroxide; diborane; dihydrogen peroxide; bromine; iron; In dichloromethane; N,N-dimethyl-formamide;