5-FLUOROBENZOFUROXAN

Base Information

Chemical Name:5-FLUOROBENZOFUROXAN
CAS No.:36389-16-9
Molecular Formula:C₆H₃FN₂O₂
Molecular Weight:154.1
Hs Code.:2934999090
Mol file:36389-16-9.mol

Synonyms:Benzofurazan,5-fluoro-, 1-oxide; 5-Fluorobenzofuroxan

Suppliers and Price of 5-FLUOROBENZOFUROXAN

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-FLUOROBENZOFUROXAN 95.00%
5MG
$ 495.68

Total 3 raw suppliers

Chemical Property of 5-FLUOROBENZOFUROXAN

Chemical Property:

Melting Point:49-50°C
Boiling Point:251.3±32.0 °C(Predicted)
PKA:3.42±0.50(Predicted)
PSA：51.49000
Density:1.63±0.1 g/cm3(Predicted)
LogP:1.39540

Purity/Quality:

99%+ ^*data from raw suppliers

5-FLUOROBENZOFUROXAN 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-FLUOROBENZOFUROXAN

There total 7 articles about 5-FLUOROBENZOFUROXAN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 364-78-3
2-nitro-4-fluoroaniline

: 36389-16-9
5-Fluorobenzofuroxan

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / CF₃CO₂H; NaNO₂; aq. NaN₃ / H₂SO₄ / 15 °C

2: acetic acid / 6 h / 100 - 110 °C

With sodium azide; trifluoroacetic acid; sodium nitrite; sulfuric acid; In acetic acid;
DOI:10.1016/S0022-1139(03)00011-3

Reference yield:

: 2369-11-1
5-fluoro-2-nitroaniline

: 36389-16-9
5-Fluorobenzofuroxan

Guidance literature:: With sodium hypochlorite; potassium hydroxide; In ethanol; water; at 0 ℃; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01748

Reference yield:

: 351-83-7
4'-fluoroacetanilide

: 36389-16-9
5-Fluorobenzofuroxan

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / HNO₃ / acetic acid / 4 h / 90 °C

2: 85 percent / CF₃CO₂H; NaNO₂; aq. NaN₃ / H₂SO₄ / 15 °C

3: acetic acid / 6 h / 100 - 110 °C

With sodium azide; nitric acid; trifluoroacetic acid; sodium nitrite; sulfuric acid; In acetic acid;
DOI:10.1016/S0022-1139(03)00011-3