C₂₀H₁₇IO₂

Base Information

• Chemical Name: C₂₀H₁₇IO₂
• CAS No.: 1444011-07-7
• Molecular Formula: C₂₀H₁₇IO₂
• Molecular Weight: 416.258
• Mol file: 1444011-07-7.mol

Synonyms:C₂₀H₁₇IO₂

Chemical Property of C₂₀H₁₇IO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₁₇IO₂

There total 2 articles about C₂₀H₁₇IO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-iodo-2,3-dimethoxybenzene (25245-33-4) → C20H17IO2 (1444011-07-7)

Guidance literature:

Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetone / 12 h / Inert atmosphere; Reflux

With boron tribromide; potassium carbonate; potassium iodide; In dichloromethane; acetone;

DOI:10.1039/c3cc42777c

Reference yield:

3-iodo-1,2-benzenediol (19337-60-1) + benzyl bromide (100-39-0) → C20H17IO2 (1444011-07-7)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 12h; Inert atmosphere; Reflux;

DOI:10.1039/c3cc42777c

Reference yield: 81.0%

C20H17IO2 (1444011-07-7) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → C26H29BO4 (1444011-09-9)

Guidance literature:

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine; In 1,4-dioxane; at 110 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c3cc42777c

upstream raw materials:

1-iodo-2,3-dimethoxybenzene

3-iodo-1,2-benzenediol

benzyl bromide

Downstream raw materials:

C₅₈H₆₂O₆

C₂₆H₂₉BO₄