4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol

Base Information

Chemical Name:4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol
CAS No.:1031400-97-1
Molecular Formula:C₁₇H₂₂F₆O₃
Molecular Weight:388.35
Hs Code.:

Synonyms:4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol

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Chemical Property of 4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol

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Technology Process of 4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol

There total 13 articles about 4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2-(benzyloxy)-5-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1,3-di-n-propylbenzene

: 1031400-97-1
4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2015.04.080

Reference yield: 72.0%

: 1031401-08-7
4-[1,1,1,3,3,3-hexafluoro-2-(methoxymethyl)oxypropan-2-yl]-2-[(1Z)-1-propenyl]-6-propylphenol

: 1031400-97-1
4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 20h;

Reference yield:

: methyl 4-(benzyloxy)-3,5-di-n-propylbenzoate

: 1031400-97-1
4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2,6-di-n-propylphenol

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water; ethanol / 2 h / Reflux

2: thionyl chloride / 2 h / 0 - 70 °C

3: tetramethylammonium fluoride / 1,2-dimethoxyethane / -78 - 20 °C / Inert atmosphere

4: sodium hydride / tetrahydrofuran / 0 - 20 °C

5: hydrogen; palladium 10% on activated carbon / methanol / 20 °C

With thionyl chloride; palladium 10% on activated carbon; tetramethylammonium fluoride; hydrogen; sodium hydride; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; water;
DOI:10.1016/j.bmcl.2015.04.080