(3S)-10-benzyloxy-1,3-decanediol

Base Information

Chemical Name:(3S)-10-benzyloxy-1,3-decanediol
CAS No.:151985-43-2
Molecular Formula:C₁₇H₂₈O₃
Molecular Weight:280.408
Hs Code.:

Synonyms:(3S)-10-benzyloxy-1,3-decanediol

Suppliers and Price of (3S)-10-benzyloxy-1,3-decanediol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3S)-10-benzyloxy-1,3-decanediol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3S)-10-benzyloxy-1,3-decanediol

There total 9 articles about (3S)-10-benzyloxy-1,3-decanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 151985-41-0
(2S,3S)-10-benzyloxy-2,3-epoxydecan-1-ol

: 151985-43-2
(3S)-10-benzyloxy-1,3-decanediol

Guidance literature:: With L-(+)-diisopropyl tartrate; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene; 1.) 0 deg C, 2 h, 2.) room temperature, 72 h;

Reference yield:

: 112-47-0
1,10-Decanediol

: 151985-43-2
(3S)-10-benzyloxy-1,3-decanediol

Guidance literature:: Multi-step reaction with 8 steps

1: 40 percent / sodium hydride / tetrahydrofuran; dimethylformamide / 1.) 0 deg C, 1 h, 2.) room temperature, 12 h

2: 68 percent / Jones reagent

3: 98 percent

4: 46 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / -78 °C

5: 74 percent / 30percent H₂O₂, sodium hydrocarbonate / tetrahydrofuran / 1.) 0 deg C, 2.) room temperature, 1 h

6: 93 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.5 h / -78 °C

7: 74 percent / tetra-iso-propyl titanate, L-(+)-diethyl tartrate, molecular sieves 3A / CH₂Cl₂ / 3 h / -25 °C

8: 40 percent / sodium bis(2-methoxyethoxy)aluminum hydride, (+)-diisopropyl tartrate / tetrahydrofuran; toluene / 1.) 0 deg C, 2 h, 2.) room temperature, 72 h

With titanium(IV) isopropylate; jones reagent; L-(+)-diisopropyl tartrate; diethyl (2R,3R)-tartrate; 3 A molecular sieve; dihydrogen peroxide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 100-44-7
benzyl chloride

: 151985-43-2
(3S)-10-benzyloxy-1,3-decanediol

Guidance literature:: Multi-step reaction with 8 steps

1: 40 percent / sodium hydride / tetrahydrofuran; dimethylformamide / 1.) 0 deg C, 1 h, 2.) room temperature, 12 h

2: 68 percent / Jones reagent

3: 98 percent

4: 46 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / -78 °C

5: 74 percent / 30percent H₂O₂, sodium hydrocarbonate / tetrahydrofuran / 1.) 0 deg C, 2.) room temperature, 1 h

6: 93 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.5 h / -78 °C

7: 74 percent / tetra-iso-propyl titanate, L-(+)-diethyl tartrate, molecular sieves 3A / CH₂Cl₂ / 3 h / -25 °C

8: 40 percent / sodium bis(2-methoxyethoxy)aluminum hydride, (+)-diisopropyl tartrate / tetrahydrofuran; toluene / 1.) 0 deg C, 2 h, 2.) room temperature, 72 h

With titanium(IV) isopropylate; jones reagent; L-(+)-diisopropyl tartrate; diethyl (2R,3R)-tartrate; 3 A molecular sieve; dihydrogen peroxide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;