5-chloro-2-dichloroacetamidobenzophenone

Base Information

• Chemical Name: 5-chloro-2-dichloroacetamidobenzophenone
• CAS No.: 17387-32-5
• Molecular Formula: C₁₅H₁₀Cl₃NO₂
• Molecular Weight: 342.609

Synonyms:5-chloro-2-dichloroacetamidobenzophenone

Chemical Property of 5-chloro-2-dichloroacetamidobenzophenone

Chemical Property:

Purity/Quality:

95%+ or 98%+ ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-chloro-2-dichloroacetamidobenzophenone

There total 2 articles about 5-chloro-2-dichloroacetamidobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

5-chloro-2-trichloroacetylaminobenzophenone (26381-66-8) + cyclohexylamine (108-91-8,157973-60-9) → 5-chloro-2-dichloroacetamidobenzophenone (17387-32-5) + 1-(2-benzoyl-4-chlorophenyl)-3-cyclohexylurea (25514-22-1) + 5-chloro-2-aminobenzophenone (719-59-5) + 6-chloro-3-cyclohexyl-3,4-dihydro-4-hydroxy-4-phenyl-2(1H)-quinazolinone (80170-81-6)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; at 100 ℃; for 7h; Further byproducts given;

DOI:10.1248/cpb.29.2135

Reference yield:

→ 5-chloro-2-dichloroacetamidobenzophenone (17387-32-5)

Guidance literature:

Erwaermen von 2-Amino-5-chlor-benzophenon in Chlf. u. Dichloracetylchlorid;

DOI:10.1139/v68-069

upstream raw materials:

5-chloro-2-trichloroacetylaminobenzophenone

cyclohexylamine

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