(MIDA boryl)(4-fluorophenyl)methyl isocyanate

Base Information

Chemical Name:(MIDA boryl)(4-fluorophenyl)methyl isocyanate
CAS No.:1380504-16-4
Molecular Formula:C₁₃H₁₂BFN₂O₅
Molecular Weight:306.058
Hs Code.:

Synonyms:(MIDA boryl)(4-fluorophenyl)methyl isocyanate

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Chemical Property of (MIDA boryl)(4-fluorophenyl)methyl isocyanate

Chemical Property:

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Technology Process of (MIDA boryl)(4-fluorophenyl)methyl isocyanate

There total 3 articles about (MIDA boryl)(4-fluorophenyl)methyl isocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1380504-04-0
2-(MIDA boryl)-2-(4-fluorophenyl)acetic acid

: 1380504-16-4
(MIDA boryl)(4-fluorophenyl)methyl isocyanate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In acetonitrile; at 50 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja304173d

Reference yield: 62.0%

: 26386-88-9
diphenyl phosphoryl azide

: 1380504-04-0
2-(MIDA boryl)-2-(4-fluorophenyl)acetic acid

: 1380504-16-4
(MIDA boryl)(4-fluorophenyl)methyl isocyanate

Guidance literature:: With triethylamine; In acetonitrile; boryl acid, azide-compound, N(C2H5)3, anhyd. CH3CN, 50°C, 1 h; silica gel chromy.;
DOI:10.1021/ja304173d

Reference yield:

: 1329422-57-2
N-methyliminodiacetyl (1-(4-fluorophenyl)-2-oxoethyl)boronate

: 1380504-16-4
(MIDA boryl)(4-fluorophenyl)methyl isocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol; cyclohexene / 20 °C

2: diphenyl phosphoryl azide; triethylamine / acetonitrile / 1 h / 50 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; diphenyl phosphoryl azide; triethylamine; In water; acetonitrile; tert-butyl alcohol; cyclohexene; 2: Curtius rearrangement;
DOI:10.1021/ja304173d