(O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten

Base Information

Chemical Name:(O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten
CAS No.:125829-08-5
Molecular Formula:C₂₅H₁₇O₇PW
Molecular Weight:644.23
Hs Code.:

Synonyms:(O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten

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Chemical Property of (O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten

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Technology Process of (O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten

There total 2 articles about (O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 125828-96-8
(Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

: 100-52-7
benzaldehyde

: 125829-08-5
(O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten

Guidance literature:: With C₆H₅COOH; In tetrahydrofuran; reaction of benzaldehyde with (phosphoranylidenephosphine)pentacarbonyltungsten complex in the presence of an excess of benzoic acid at 25°C for 5 min; evapn. of the solvent, chromy. (hexane/CH2Cl2), elem. anal.;
DOI:10.1021/ja00162a051

Reference yield:

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 125829-08-5
(O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: C₆H₅COOH / tetrahydrofuran

With C₆H₅COOH; In tetrahydrofuran;
DOI:10.1021/ja00162a051