(Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

Base Information

Chemical Name:(Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten
CAS No.:125828-96-8
Molecular Formula:C₂₃H₃₂O₅P₂W
Molecular Weight:634.302
Hs Code.:

Synonyms:(Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

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Chemical Property of (Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

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Technology Process of (Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

There total 1 articles about (Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 998-40-3
tributylphosphine

: 125828-96-8
(Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

: 17649-59-1
dimethyl 4,5-dimethylphthalate

Guidance literature:: In tetrahydrofuran; addn. of tributylphosphine to a soln. of phosphanorbornadiene complex in THF, stirring 5 h at 25°C; monitored by (31)P-NMR;
DOI:10.1021/ja00162a051

Reference yield: 80.0%

: 125828-96-8
(Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

: 100-52-7
benzaldehyde

: 125829-08-5
(O-benzoyl phenylbenzylphosphinite)pentacarbonyltungsten

Guidance literature:: With C₆H₅COOH; In tetrahydrofuran; reaction of benzaldehyde with (phosphoranylidenephosphine)pentacarbonyltungsten complex in the presence of an excess of benzoic acid at 25°C for 5 min; evapn. of the solvent, chromy. (hexane/CH2Cl2), elem. anal.;
DOI:10.1021/ja00162a051

Reference yield: 75.0%

: 125828-96-8
(Ph)(tributyl)(phosphoranylidenephosphine)pentacarbonyltungsten

: 100-52-7
benzaldehyde

: 125829-01-8
(o-methyl phenylbenzylphosphinite)pentacarbonyltungsten

Guidance literature:: With CH₃OH; In tetrahydrofuran; reaction of benzaldehyde with phosphanorbornadiene complex in presence of an excess of MeOH at 25°C for 5 min,; evapn. of the solvent, chromy (hexane), elem. anal.;
DOI:10.1021/ja00162a051