phenyl 5-chloro-2-nitrophenylmethanesulfonate

Base Information

Chemical Name:phenyl 5-chloro-2-nitrophenylmethanesulfonate
CAS No.:115663-35-9
Molecular Formula:C₁₃H₁₀ClNO₅S
Molecular Weight:327.745
Hs Code.:

Synonyms:phenyl 5-chloro-2-nitrophenylmethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 5-chloro-2-nitrophenylmethanesulfonate

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Technology Process of phenyl 5-chloro-2-nitrophenylmethanesulfonate

There total 2 articles about phenyl 5-chloro-2-nitrophenylmethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 16764-29-7
chloro-methanesulfonic acid phenyl ester

: 100-00-5
4-chlorobenzonitrile

: 115663-35-9
phenyl 5-chloro-2-nitrophenylmethanesulfonate

Guidance literature:: With sodium hydroxide; In dimethyl sulfoxide; for 1h; Ambient temperature;
DOI:10.1055/s-1983-30611

Reference yield:

: 108-95-2,27073-41-2
phenol

: 115663-35-9
phenyl 5-chloro-2-nitrophenylmethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOH / 2.) tetrabutylammonium bromide / 1.) water, 2.) CHCl₃, 30 min

2: 67 percent / NaOH / dimethylsulfoxide / 1 h / Ambient temperature

With sodium hydroxide; tetrabutylammomium bromide; In dimethyl sulfoxide;
DOI:10.1055/s-1983-30611

Reference yield:

: 115663-35-9
phenyl 5-chloro-2-nitrophenylmethanesulfonate

: 105-36-2
ethyl bromoacetate

: 115663-41-7
5-chloro-2-nitro-cinnamic acid ethyl ester

: 115663-42-8
(Z)-3-(5-Chloro-2-nitro-phenyl)-acrylic acid ethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 8h; Yield given. Yields of byproduct given;
DOI:10.1055/s-1987-28280