C₂₉H₃₀N₄O₁₀S

Base Information

Chemical Name:C₂₉H₃₀N₄O₁₀S
CAS No.:1004524-47-3
Molecular Formula:C₂₉H₃₀N₄O₁₀S
Molecular Weight:626.644
Hs Code.:

C<sub>29</sub>H<sub>30</sub>N<sub>4</sub>O<sub>10</sub>S

Synonyms:C₂₉H₃₀N₄O₁₀S

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Chemical Property of C₂₉H₃₀N₄O₁₀S

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Technology Process of C₂₉H₃₀N₄O₁₀S

There total 9 articles about C₂₉H₃₀N₄O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1004524-46-2
C₂₃H₂₇N₃O₆

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1004524-47-3
C₂₉H₃₀N₄O₁₀S

Guidance literature:: With triethylamine; In acetonitrile; at 0 ℃; for 3h;

Reference yield:

: 32462-30-9
(S)-hydroxyphenylglycine

: 1004524-47-3
C₂₉H₃₀N₄O₁₀S

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydrogencarbonate / acetone; water

2: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0 - 20 °C

3: potassium carbonate / acetone / 17 h / Inert atmosphere; Reflux

4: silver sulfate; iodine / methanol / 0.5 h

5: lithium hydroxide / water; tetrahydrofuran

6: sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile / Inert atmosphere

7: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / acetonitrile / 21 h / 80 °C / Sealed tube; Inert atmosphere

8: trifluoroacetic acid / dichloromethane / 0.83 h / Inert atmosphere

9: triethylamine / acetonitrile / 2 h

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iodine; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 69651-48-5
N-tert-butyloxycarbonyl-L-4-hydroxyphenylglycine

: 1004524-47-3
C₂₉H₃₀N₄O₁₀S

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0 - 20 °C

2: potassium carbonate / acetone / 17 h / Inert atmosphere; Reflux

3: silver sulfate; iodine / methanol / 0.5 h

4: lithium hydroxide / water; tetrahydrofuran

5: sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile / Inert atmosphere

6: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / acetonitrile / 21 h / 80 °C / Sealed tube; Inert atmosphere

7: trifluoroacetic acid / dichloromethane / 0.83 h / Inert atmosphere

8: triethylamine / acetonitrile / 2 h

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iodine; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;