N⁽²⁾-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin

Base Information

• Chemical Name: N⁽²⁾-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin
• CAS No.: 1225517-13-4
• Molecular Formula: C₁₈H₁₉N₇O₄
• Molecular Weight: 397.393

Synonyms:N⁽²⁾-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin

Chemical Property of N⁽²⁾-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin

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Technology Process of N⁽²⁾-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin

There total 1 articles about N⁽²⁾-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

6-[(acetykoxy)methyl]-2-{[(dimethylamino)methylene]amino}-3-[2-(4-nitrophenyl)ethyl]pteridin-4(3H)-one (522614-28-4) → N(2)-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin (1225517-13-4)

Guidance literature:

6-[(acetykoxy)methyl]-2-{[(dimethylamino)methylene]amino}-3-[2-(4-nitrophenyl)ethyl]pteridin-4(3H)-one; With sodium methylate; In methanol; dichloromethane; at 0 - 20 ℃;

In water; at 20 ℃; for 24h;

DOI:10.3987/COM-09-S(S)78

Reference yield: 93.0%

2,3,4,6-tetra-O-benzoylglucosyl bromide (14218-11-2) + N(2)-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin (1225517-13-4) → 3,4,6-tri-O-benzoyl-α-D-glucopyranose-1,2-{[N(2)-(N,N-dimethylaminomethylene)-3-(4-nitrophenylethyl)pterin-6-yl]methyl}orthobenzoate

Guidance literature:

With tetraethylammonium bromide; N-ethyl-N,N-diisopropylamine; In chloroform; for 42h; Reflux;

DOI:10.3987/COM-09-S(S)78

Reference yield: 69.0%

4,6-di-O-acetyl-2,3-di-O-(4-methoxybenzyl)-α-D-glucopyranosyl bromide (1146498-54-5) + N(2)-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin (1225517-13-4) → N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-{[4,6-di-O-acetyl-2,3-di-O-(4-methoxybenzyl)-α-D-glycopyranosyloxy]methyl}pterin

Guidance literature:

With tetraethylammonium bromide; N-ethyl-N,N-diisopropylamine; In chloroform; for 24h; Reflux;

DOI:10.3987/COM-09-S(S)78

upstream raw materials:

6-[(acetykoxy)methyl]-2-{[(dimethylamino)methylene]amino}-3-[2-(4-nitrophenyl)ethyl]pteridin-4(3H)-one

Downstream raw materials:

N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin

6-benzoyloxy-N⁽²⁾-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]pterin

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