C₃₃H₄₈O₁₀

Base Information

Chemical Name:C₃₃H₄₈O₁₀
CAS No.:1449602-80-5
Molecular Formula:C₃₃H₄₈O₁₀
Molecular Weight:604.738
Hs Code.:

C<sub>33</sub>H<sub>48</sub>O<sub>10</sub>

Synonyms:C₃₃H₄₈O₁₀

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Chemical Property of C₃₃H₄₈O₁₀

Chemical Property:

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Technology Process of C₃₃H₄₈O₁₀

There total 3 articles about C₃₃H₄₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1449602-77-0
C₁₉H₃₅ClO₈

: 37155-50-3
2-(4-methoxybenzyl)phenol

: 1449602-80-5
C₃₃H₄₈O₁₀

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; (η4-1,5-cyclooctadiene)dichlororuthenium(II); potassium carbonate; In acetonitrile; at 60 ℃; for 48h; Inert atmosphere;
DOI:10.1002/anie.201302543

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1449602-80-5
C₃₃H₄₈O₁₀

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 96 h / 20 °C

1.2: 24 h

2.1: potassium carbonate; 1,1'-bis-(diphenylphosphino)ferrocene; (η4-1,5-cyclooctadiene)dichlororuthenium(II) / acetonitrile / 48 h / 60 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (η4-1,5-cyclooctadiene)dichlororuthenium(II); potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; acetonitrile; 1.1: |Baylis-Hillman Reaction;
DOI:10.1002/anie.201302543

Reference yield:

: 1323271-65-3
5,5a-didehydro-2,3,4,6-tetra-O-(ethoxymethyl)-5a-carba-α-D-xylohexopyranose

: 1449602-80-5
C₃₃H₄₈O₁₀

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; tetrabutyl-ammonium chloride / dichloromethane / 0.25 h / 0 °C / Molecular sieve

1.2: 3.25 h / 0 - 20 °C / Molecular sieve

2.1: potassium carbonate; 1,1'-bis-(diphenylphosphino)ferrocene; (η4-1,5-cyclooctadiene)dichlororuthenium(II) / acetonitrile / 48 h / 60 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (η4-1,5-cyclooctadiene)dichlororuthenium(II); tetrabutyl-ammonium chloride; potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/anie.201302543