phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Base Information

Chemical Name:phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate
CAS No.:1447497-27-9
Molecular Formula:C₂₈H₃₃NO₇
Molecular Weight:495.573
Hs Code.:

Synonyms:phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

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Chemical Property of phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

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Technology Process of phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

There total 8 articles about phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1447497-25-7
phenyl 4-amino-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

: 123-11-5
4-methoxy-benzaldehyde

: 1447497-27-9
phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃;
DOI:10.1021/ma4010023

Reference yield:

: 1447497-21-3
2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-4-nitrobenzoic acid

: 1447497-27-9
phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride / 0 - 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 40 h / 40 °C / 30003 Torr

4: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1021/ma4010023

Reference yield:

: 1447497-19-9
methyl 2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-4-nitrobenzoate

: 1447497-27-9
phenyl 4-((4-methoxybenzyl)amino)-2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide; water; methanol / 2 h / Reflux

2: oxalyl dichloride / 0 - 20 °C

3: triethylamine / dichloromethane / 0 - 20 °C

4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 40 h / 40 °C / 30003 Torr

5: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

With methanol; oxalyl dichloride; palladium 10% on activated carbon; water; hydrogen; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; sodium hydroxide; In dichloromethane; ethyl acetate;
DOI:10.1021/ma4010023