3,4,5-trichlorobenzyl azide

Base Information Edit

Chemical Name:3,4,5-trichlorobenzyl azide
CAS No.:1213234-83-3
Molecular Formula:C₇H₄Cl₃N₃
Molecular Weight:236.488
Hs Code.:
Mol file:1213234-83-3.mol

Synonyms:3,4,5-trichlorobenzyl azide

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Chemical Property of 3,4,5-trichlorobenzyl azide Edit

Chemical Property:

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Technology Process of 3,4,5-trichlorobenzyl azide

There total 3 articles about 3,4,5-trichlorobenzyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7520-67-4
3,4,5-trichloro-benzyl alcohol

: 1213234-83-3
3,4,5-trichlorobenzyl azide

Guidance literature:: With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; for 3.5h;

Reference yield:

: 56961-25-2
4-amino-3,5-dichlorobenzoic acid

: 1213234-83-3
3,4,5-trichlorobenzyl azide

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 10.25 h / 0 - 60 °C

1.2: 0 °C

2.1: tert.-butylnitrite; copper dichloride / acetonitrile / 1.58 h / 20 °C

3.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3.5 h / 20 °C

With lithium aluminium tetrahydride; tert.-butylnitrite; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper dichloride; In tetrahydrofuran; toluene; acetonitrile;

Reference yield:

: 74878-32-3
4-amino-3,5-dichlorobenzyl alcohol

: 1213234-83-3
3,4,5-trichlorobenzyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: tert.-butylnitrite; copper dichloride / acetonitrile / 1.58 h / 20 °C

2: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 3.5 h / 20 °C

With tert.-butylnitrite; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper dichloride; In toluene; acetonitrile;