C₃₂H₃₆Br₂O

Base Information

• Chemical Name: C₃₂H₃₆Br₂O
• CAS No.: 1616870-40-6
• Molecular Formula: C₃₂H₃₆Br₂O
• Molecular Weight: 596.445
• Mol file: 1616870-40-6.mol

Synonyms:C₃₂H₃₆Br₂O

Chemical Property of C₃₂H₃₆Br₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₃₆Br₂O

There total 3 articles about C₃₂H₃₆Br₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1 ,6-dibromohexane (629-03-8) + 2-benzoylfluorene (15860-31-8) → C32H36Br2O (1616870-40-6)

Guidance literature:

With tetrabutylammomium bromide; sodium hydroxide; In water; at 75 ℃; for 12h;

DOI:10.1039/c4tb00367e

Reference yield:

9H-fluorene (86-73-7) → C32H36Br2O (1616870-40-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / carbon disulfide / Inert atmosphere; Cooling with ice

1.2: 12 h / Reflux

2.1: tetrabutylammomium bromide; sodium hydroxide / water / 12 h / 75 °C

With aluminum (III) chloride; tetrabutylammomium bromide; sodium hydroxide; In carbon disulfide; water;

DOI:10.1039/c4tb00367e

Reference yield:

benzoyl chloride (98-88-4) → C32H36Br2O (1616870-40-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / carbon disulfide / Inert atmosphere; Cooling with ice

1.2: 12 h / Reflux

2.1: tetrabutylammomium bromide; sodium hydroxide / water / 12 h / 75 °C

With aluminum (III) chloride; tetrabutylammomium bromide; sodium hydroxide; In carbon disulfide; water;

DOI:10.1039/c4tb00367e

upstream raw materials:

9H-fluorene

benzoyl chloride

1 ,6-dibromohexane

2-benzoylfluorene

Downstream raw materials:

1,2-bis[9,9-bis(6-bromohexyl)-2-fluorenyl]-1,2-diphenylethene