4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane

Base Information

Chemical Name:4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane
CAS No.:126764-96-3
Molecular Formula:C₂₅H₃₆O₃Si
Molecular Weight:412.645
Hs Code.:

Synonyms:4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane

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Chemical Property of 4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane

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Technology Process of 4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane

There total 4 articles about 4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 127793-62-8
4-((tert-butyldiphenylsilyl)oxy)butanal

: 42075-32-1
(2R,4R)-pentanediol

: 126764-96-3
4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 2h; Heating;
DOI:10.1039/P19910003307

Reference yield:

: 130372-07-5
4-(tret-butyldiphenylsilyloxy)butan-1-ol

: 126764-96-3
4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl chloride, 2.) Et₃N / 1.) CH₂Cl₂, DMSO, -70 deg C, 25 min 2.) r.t.

2: 99 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating

With oxalyl dichloride; toluene-4-sulfonic acid; triethylamine; In benzene;
DOI:10.1039/P19910003307

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 126764-96-3
4-<(4R,6R)-4,6-Dimethyl-1,3-dioxan-2-yl>-1-tert-butyldiphenylsilyloxypropane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, r.t., 1 h, 2.) r.t., 1.5 h

2: 1.) oxalyl chloride, 2.) Et₃N / 1.) CH₂Cl₂, DMSO, -70 deg C, 25 min 2.) r.t.

3: 99 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating

With oxalyl dichloride; sodium hydride; toluene-4-sulfonic acid; triethylamine; In benzene;
DOI:10.1039/P19910003307