methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester

Base Information

Chemical Name:methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester
CAS No.:1020852-38-3
Molecular Formula:C₁₆H₂₃NO₆S
Molecular Weight:357.428
Hs Code.:

Synonyms:methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester

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Technology Process of methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester

There total 1 articles about methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1020852-36-1
tert-butyl ((S)-2-hydroxy-3-phenylpropionylamino)acetate

: 124-63-0
methanesulfonyl chloride

: 1020852-38-3
methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2008.01.103

Reference yield: 82.0%

: 1020852-38-3
methanesulfonic acid (S)-1-benzyl-2-[(tert-butoxycarbonyl)methylamino]-2-oxoethyl ester

: 1020852-40-7
tert-butyl ((R)-2-azido-3-phenylpropionylamino)acetate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; dmap; sodium azide; 2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin; In dichloromethane; for 24h; Heating;
DOI:10.1016/j.tet.2008.01.103