(E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate

Base Information

Chemical Name:(E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate
CAS No.:1374767-32-4
Molecular Formula:C₂₁H₂₉ClO₅
Molecular Weight:396.911
Hs Code.:

Synonyms:(E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate

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Chemical Property of (E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate

Chemical Property:

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Technology Process of (E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate

There total 11 articles about (E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₂₃BrO₂

: 83324-59-8
3-chloro-4,6-dihydroxy-2-methyl-benzaldehyde

: 1374767-32-4
(E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate

Guidance literature:: With calcium(II) chloride dihydrate; potassium hydroxide; In methanol; at 0 - 20 ℃; for 18h;

Reference yield:

: 629-11-8
1,6-hexanediol

: 1374767-32-4
(E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate

Guidance literature:: Multi-step reaction with 10 steps

1.1: 1H-imidazole; dmap / toluene; N,N-dimethyl-formamide / 15 h / 0 - 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / chloroform / 2 h / -60 °C / Inert atmosphere

2.2: 1 h / -60 °C

3.1: methyllithium / tetrahydrofuran; diethyl ether / 1 h / -15 - 20 °C

3.2: 20 h / -15 - 20 °C

4.1: diisobutylaluminium hydride / hexane; toluene / 3 h / -85 - -65 °C

5.1: pyridine / 16 h / 20 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

7.1: triethylamine; dmap / chloroform / 20 h / 0 - 20 °C

8.1: sodium methylate; guanidine hydrochloride / chloroform; methanol / 5 h / 20 °C / Inert atmosphere

9.1: triphenylphosphine; carbon tetrabromide / chloroform / 1.5 h / 0 °C

10.1: calcium(II) chloride dihydrate; potassium hydroxide / methanol / 18 h / 0 - 20 °C

With pyridine; 1H-imidazole; dmap; oxalyl dichloride; calcium(II) chloride dihydrate; carbon tetrabromide; tetrabutyl ammonium fluoride; methyllithium; guanidine hydrochloride; sodium methylate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; N,N-dimethyl-formamide; toluene; 2.1: |Swern Oxidation;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 1374767-32-4
(E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-6-octenyl pivalate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; dmap / chloroform / 20 h / 0 - 20 °C

2: sodium methylate; guanidine hydrochloride / chloroform; methanol / 5 h / 20 °C / Inert atmosphere

3: triphenylphosphine; carbon tetrabromide / chloroform / 1.5 h / 0 °C

4: calcium(II) chloride dihydrate; potassium hydroxide / methanol / 18 h / 0 - 20 °C

With dmap; calcium(II) chloride dihydrate; carbon tetrabromide; guanidine hydrochloride; sodium methylate; triethylamine; triphenylphosphine; potassium hydroxide; In methanol; chloroform;