3,4-dimethoxyphenacyl azide ethylene ketal

Base Information

Chemical Name:3,4-dimethoxyphenacyl azide ethylene ketal
CAS No.:947594-79-8
Molecular Formula:C₁₂H₁₅N₃O₄
Molecular Weight:265.269
Hs Code.:

Synonyms:3,4-dimethoxyphenacyl azide ethylene ketal

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Chemical Property of 3,4-dimethoxyphenacyl azide ethylene ketal

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Technology Process of 3,4-dimethoxyphenacyl azide ethylene ketal

There total 2 articles about 3,4-dimethoxyphenacyl azide ethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 187101-52-6
2-azido-1-(3,4-dimethoxyphenyl)ethanone

: 107-21-1
ethylene glycol

: 947594-79-8
3,4-dimethoxyphenacyl azide ethylene ketal

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃;
DOI:10.1021/jm0703035

Reference yield:

: 1835-02-5
2-Bromo-1-(3,4-dimethoxyphenyl)ethanone

: 947594-79-8
3,4-dimethoxyphenacyl azide ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / sodium azide / dimethylsulfoxide / 20 °C

2: 80 percent / boron trifluoride etherate / CH₂Cl₂ / 20 °C

With sodium azide; boron trifluoride diethyl etherate; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm0703035

Reference yield: 85.0%

: 947594-79-8
3,4-dimethoxyphenacyl azide ethylene ketal

: 109224-71-7
2-(aminomethyl)-2-(3,4-dimethoxyphenyl)-1,2-dioxolane

Guidance literature:: 3,4-dimethoxyphenacyl azide ethylene ketal; With triphenylphosphine; In tetrahydrofuran;

With water; In tetrahydrofuran; Further stages.;
DOI:10.1021/jm0703035