[2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II)

Base Information

• Chemical Name: [2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II)
• CAS No.: 134776-88-8
• Molecular Formula: C₄₄H₁₂Cl₁₆N₄Zn
• Molecular Weight: 1229.24

Synonyms:[2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II)

Chemical Property of [2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II)

Chemical Property:

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Technology Process of [2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II)

There total 6 articles about [2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato] zinc(II) (100506-72-7) → [2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II) (134776-88-8)

Guidance literature:

With N-chloro-succinimide; In chloroform; butan-1-ol; at 20 ℃; for 0.5h; Solvent; Reflux;

DOI:10.1134/S1070363220110122

Reference yield: 31.4%

N-chloro-succinimide (128-09-6) + [5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato] zinc(II) (100506-72-7) → [2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II) (134776-88-8)

Guidance literature:

aluminium trichloride; In further solvent(s); refluxing 0.42 mmol of Zn(C20H8N4(C6H3Cl2)4), 7.5 mmol of N-Cl-succinimide and 6 mg of AlCl3 for 6 hours in 200 ml 1,2-dichloroethane and evaporation;; flash chromatography (silica gel, 1:1 CH2Cl2/petroleum ether); detn. by (1)H NMR and UV spectroscopy;;

Reference yield:

C44H19Cl8N4Zn → [2,3,7,8,12,13,17,18-octachloro-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato]zinc(II) (134776-88-8)

Guidance literature:

With N-chloro-succinimide; In methanol; for 11h; Reflux;

upstream raw materials:

N-chloro-succinimide

[5,10,15,20-tetrakis(2,6-dichlorophenyl)porphyrinato] zinc(II)

2,6-dichlorobenzaldehyde

zinc diacetate

Downstream raw materials:

C₄₄H₁₂Cl₁₆FeN₄⁽¹⁺⁾*Cl^(1-)

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