1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole

Base Information

Chemical Name:1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole
CAS No.:1325725-21-0
Molecular Formula:C₁₁H₁₁N₃O
Molecular Weight:201.228
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole

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Chemical Property of 1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole

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Technology Process of 1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole

There total 11 articles about 1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2101-87-3
p-methoxy-phenylazide

: 927-74-2
3-Butyn-1-ol

: 1325725-21-0
1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole

Guidance literature:: 3-Butyn-1-ol; With triethylamine; In dichloromethane; at 20 ℃; polystyrene Inert atmosphere;

p-methoxy-phenylazide; With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; at 20 ℃; polystyrene Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In N,N-dimethyl-formamide; at 120 ℃; for 1h; polystyrene Inert atmosphere;
DOI:10.1080/00397911.2015.1130228

Reference yield: 88.0%

: 38771-21-0
4-bromobut-1-yne

: 2101-87-3
p-methoxy-phenylazide

: 1325725-21-0
1-(4-methoxyphenyl)-4-vinyl-1H-1,2,3-triazole

Guidance literature:: 4-bromobut-1-yne; p-methoxy-phenylazide; With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In ethanol; water; at 25 ℃; for 12h; Green chemistry;

With sodium hydroxide; In ethanol; water; at 45 ℃; for 8h; Green chemistry;
DOI:10.1039/c3gc37066f