C₂₅H₃₆F₄N₄O₁₁S

Base Information

• Chemical Name: C₂₅H₃₆F₄N₄O₁₁S
• CAS No.: 1309456-99-2
• Molecular Formula: C₂₅H₃₆F₄N₄O₁₁S
• Molecular Weight: 676.641
• Mol file: 1309456-99-2.mol

Synonyms:C₂₅H₃₆F₄N₄O₁₁S

Chemical Property of C₂₅H₃₆F₄N₄O₁₁S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₃₆F₄N₄O₁₁S

There total 9 articles about C₂₅H₃₆F₄N₄O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → C25H36F4N4O11S (1309456-99-2)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium hydride / mineral oil / 1.5 h / 20 °C / Inert atmosphere

2: sodium iodide / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere

3: N,N-dimethyl-formamide / 1 h / 50 °C / Inert atmosphere

4: palladium on carbon; hydrogen / methanol / 1 h / 20 °C

5: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere

With palladium on carbon; hydrogen; sodium hydride; sodium iodide; In methanol; N,N-dimethyl-formamide; mineral oil;

DOI:10.1039/c1ob05040k

Reference yield:

C18H35N3O10S (1309457-05-3) → C25H36F4N4O11S (1309456-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on carbon; hydrogen / methanol / 1 h / 20 °C

2: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere

With palladium on carbon; hydrogen; In methanol; N,N-dimethyl-formamide;

DOI:10.1039/c1ob05040k

Reference yield:

2-[2-(chloroethoxy)ethoxy]ethanol (5197-62-6) → C25H36F4N4O11S (1309456-99-2)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium azide / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

2: sodium hydride / mineral oil / 1.5 h / 20 °C / Inert atmosphere

3: sodium iodide / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere

4: N,N-dimethyl-formamide / 1 h / 50 °C / Inert atmosphere

5: palladium on carbon; hydrogen / methanol / 1 h / 20 °C

6: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere

With sodium azide; palladium on carbon; hydrogen; sodium hydride; sodium iodide; In methanol; N,N-dimethyl-formamide; mineral oil;

DOI:10.1039/c1ob05040k

upstream raw materials:

2[-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl p-tosylate

sodium salt of 1-thio-α-D-mannose

1-azido-17-iodo-3,6,9,12,15-pentaoxaheptadecane

C₁₈H₃₅N₃O₁₀S