(2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

Base Information

Chemical Name:(2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol
CAS No.:860640-74-0
Molecular Formula:C₁₈H₂₅N₁₅O₇
Molecular Weight:563.493
Hs Code.:

(2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

Synonyms:(2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

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Chemical Property of (2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

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Technology Process of (2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

There total 8 articles about (2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 860640-72-8
Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

: 485809-80-1
4-azido-2,3-di-O-acetyl-4,6-dideoxy-α-D-glucopyranosyl trichloroacetimidate

: 860640-74-0
(2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

Guidance literature:: Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester; 4-azido-2,3-di-O-acetyl-4,6-dideoxy-α-D-glucopyranosyl trichloroacetimidate; With boron trifluoride diethyl etherate; In dichloromethane;

With sodium methylate; In methanol;

Reference yield:

: Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-((2S,3R,4S,5R,6R)-3,4-diacetoxy-5-azido-6-methyl-tetrahydro-pyran-2-yloxy)-cyclohexyl ester

: 860640-74-0
(2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

Guidance literature:: With sodium methylate; In methanol; at 20 ℃;
DOI:10.1081/CAR-200059968

Reference yield:

: 860640-70-6
1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

: 860640-74-0
(2S,3R,4S,5S,6R)-5-Azido-2-[(1R,2R,3S,5R,6S)-3,5-diazido-2-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-6-hydroxy-cyclohexyloxy]-6-methyl-tetrahydro-pyran-3,4-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / N,N-diisopropylethylamine / CH₂Cl₂ / -50 °C

2: BF₃*Et₂O; molecular sieves 4 Angstroem / CH₂Cl₂ / 0.75 h / -50 °C

3: 0.16 g / sodium methoxide / methanol / 20 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; sodium methylate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1081/CAR-200059968