Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

Base Information

Chemical Name:Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester
CAS No.:860640-72-8
Molecular Formula:C₁₉H₂₀N₁₂O₅
Molecular Weight:496.445
Hs Code.:

Synonyms:Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

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Chemical Property of Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

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Technology Process of Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

There total 5 articles about Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 860640-70-6
1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

: 98-88-4
benzoyl chloride

: 860640-72-8
Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -50 ℃;
DOI:10.1081/CAR-200059968

Reference yield:

: 860640-71-7
C₁₈H₂₄N₁₂O₄

: 860640-72-8
Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / acetic acid / H₂O; dioxane / 24 h / 65 °C

2: 85 percent / N,N-diisopropylethylamine / CH₂Cl₂ / -50 °C

With acetic acid; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water;
DOI:10.1081/CAR-200059968

Reference yield:

: 1053694-75-9
C₂₀H₂₄F₆N₁₂O₁₀S₂

: 860640-72-8
Benzoic acid (1S,2S,3R,4S,6R)-4,6-diazido-3-((2R,3R,6S)-3-azido-6-azidomethyl-3,6-dihydro-2H-pyran-2-yloxy)-2-hydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 0.39 g / sodium iodide; sodium thiosulfate / acetone / 20 °C

2: 95 percent / acetic acid / H₂O; dioxane / 24 h / 65 °C

3: 85 percent / N,N-diisopropylethylamine / CH₂Cl₂ / -50 °C

With sodium thiosulfate; acetic acid; N-ethyl-N,N-diisopropylamine; sodium iodide; In 1,4-dioxane; dichloromethane; water; acetone;
DOI:10.1081/CAR-200059968