(E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran

Base Information

Chemical Name:(E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran
CAS No.:1240254-45-8
Molecular Formula:C₃₁H₂₆O₄
Molecular Weight:462.545
Hs Code.:

Synonyms:(E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran

Chemical Property:

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Technology Process of (E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran

There total 6 articles about (E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1145-93-3
diethyl 4-methoxybenzylphosphonate

: C₂₃H₁₈O₄

: 1240254-45-8
(E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 120 ℃; for 0.5h; Microwave irradiation;
DOI:10.1002/adsc.201601089

Reference yield:

: C₁₆H₁₂O₃

: 1240254-45-8
(E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; palladium diacetate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid / N,N-dimethyl acetamide / 20 h / 100 °C

2: sodium hydride / tetrahydrofuran / 0.5 h / 120 °C / Microwave irradiation

With palladium diacetate; sodium hydride; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In tetrahydrofuran; N,N-dimethyl acetamide; 2: |Wittig-Horner Reaction;
DOI:10.1002/adsc.201601089

Reference yield:

: 19520-74-2
3-hydroxy-5-methoxy-benzoic acid methyl ester

: 1240254-45-8
(E)-6-methoxy-2-(4-methoxyphenyl)-4-(4-methoxystyryl)-3-phenylbenzofuran

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / acetone / 2 h / Reflux

2: bismuth(lll) trifluoromethanesulfonate / dichloromethane / 20 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C

4: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

5: potassium carbonate; palladium diacetate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid / N,N-dimethyl acetamide / 20 h / 100 °C

6: sodium hydride / tetrahydrofuran / 0.5 h / 120 °C / Microwave irradiation

With bismuth(lll) trifluoromethanesulfonate; lithium aluminium tetrahydride; palladium diacetate; sodium hydride; potassium carbonate; Dess-Martin periodane; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; acetone; 6: |Wittig-Horner Reaction;
DOI:10.1002/adsc.201601089