{2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone

Base Information

Chemical Name:{2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone
CAS No.:752243-41-7
Molecular Formula:C₃₁H₃₅N₃O₆S
Molecular Weight:577.701
Hs Code.:

Synonyms:{2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone

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Chemical Property of {2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone

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Technology Process of {2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone

There total 6 articles about {2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450914-73-4
C₃₃H₃₉N₃O₆S

: 752243-41-7
{2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone

Guidance literature:: C₃₃H₃₉N₃O₆S; With sodium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 24h;

With hydrogenchloride; In water; at 20 ℃; for 2h;

Reference yield:

: 7304-32-7
2-fluoro-5-nitrobenzoic acid

: 752243-41-7
{2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: (COCl)2 / toluene; dimethylformamide / 20 °C

2.1: Et₃N / tetrahydrofuran

3.1: Zn; AcOH

4.1: NaNO₂; HCl; AcOH

4.2: SO₂; CuCl₂; aq. AcOH

4.3: aq. Na₂CO₃ / dioxane

5.1: dimethylsulfoxide / 120 °C

With hydrogenchloride; oxalyl dichloride; acetic acid; triethylamine; zinc; sodium nitrite; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm049747g

Reference yield:

: 709-46-6
2-fluoro-5-nitrobenzoyl chloride

: 752243-41-7
{2-(2,2-diphenyl-ethylamino)-5-[4-(4-carboxy)-piperidine-1-sulfonyl]-phenyl}-morpholin-4-yl-methanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₃N / tetrahydrofuran

2.1: Zn; AcOH

3.1: NaNO₂; HCl; AcOH

3.2: SO₂; CuCl₂; aq. AcOH

3.3: aq. Na₂CO₃ / dioxane

4.1: dimethylsulfoxide / 120 °C

With hydrogenchloride; acetic acid; triethylamine; zinc; sodium nitrite; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jm049747g