C₁₄H₁₅Cl₂NO₃

Base Information

Chemical Name:C₁₄H₁₅Cl₂NO₃
CAS No.:1268246-39-4
Molecular Formula:C₁₄H₁₅Cl₂NO₃
Molecular Weight:316.184
Hs Code.:

C<sub>14</sub>H<sub>15</sub>Cl<sub>2</sub>NO<sub>3</sub>

Synonyms:C₁₄H₁₅Cl₂NO₃

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Chemical Property of C₁₄H₁₅Cl₂NO₃

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Technology Process of C₁₄H₁₅Cl₂NO₃

There total 12 articles about C₁₄H₁₅Cl₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1268246-38-3
C₂₀H₂₉Cl₂NO₃Si

: 1268246-39-4
C₁₄H₁₅Cl₂NO₃

Guidance literature:: C₂₀H₂₉Cl₂NO₃Si; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -5 - 0 ℃; for 3.5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran;

Reference yield:

: 278597-30-1
[3-(2,6-dichlorophenyl)-5-(propan-2-yl)-1,2-oxazol-4-yl]methanol

: 1268246-39-4
C₁₄H₁₅Cl₂NO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: N-Bromosuccinimide / tetrachloromethane / 1 h / Reflux

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C

3.2: 0.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

5.1: osmium(VIII) oxide; 2,6-dimethylpyridine; sodium periodate / 1,4-dioxane; water / 2 h / 20 °C

6.1: tetrahydrofuran / 3.5 h / -30 - -20 °C / Inert atmosphere

7.1: toluene-4-sulfonic acid / diethyl ether; tetrahydrofuran / 0 - 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3.5 h / -5 - 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium periodate; N-Bromosuccinimide; osmium(VIII) oxide; tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; diethyl ether; dichloromethane; water;

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 1268246-39-4
C₁₄H₁₅Cl₂NO₃

Guidance literature:: Multi-step reaction with 12 steps

1.1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 24 h / 90 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 16 h / 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

4.2: 0.17 h / 0 °C

5.1: triethylamine / dichloromethane / 20 °C

6.1: N-Bromosuccinimide / tetrachloromethane / 1 h / Reflux

7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C

7.2: 0.5 h / 20 °C

8.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

9.1: osmium(VIII) oxide; 2,6-dimethylpyridine; sodium periodate / 1,4-dioxane; water / 2 h / 20 °C

10.1: tetrahydrofuran / 3.5 h / -30 - -20 °C / Inert atmosphere

11.1: toluene-4-sulfonic acid / diethyl ether; tetrahydrofuran / 0 - 20 °C

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3.5 h / -5 - 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; osmium(VIII) oxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;