1,3,6,8-TETRAKIS(TERT-BUTYL)CARBAZOLE

Base Information

• Chemical Name: 1,3,6,8-TETRAKIS(TERT-BUTYL)CARBAZOLE
• CAS No.: 34601-54-2
• Molecular Formula: C28H41 N
• Molecular Weight: 391.63
• Hs Code.: 2933990090
• Mol file: 34601-54-2.mol

Synonyms:TOSLAB 97919;1,3,6,8-TETRAKIS(TERT-BUTYL)CARBAZOLE

Chemical Property of 1,3,6,8-TETRAKIS(TERT-BUTYL)CARBAZOLE

Chemical Property:

• Vapor Pressure: 7.62E-09mmHg at 25°C
• Melting Point: 189.0 to 193.0 °C
• Refractive Index: 1.558
• Boiling Point: 478.2°C at 760 mmHg
• Flash Point: 196.7°C
• PSA: 15.79000
• Density: 0.972g/cm³
• LogP: 8.51110
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99%min ^*data from raw suppliers

1,3,6,8-Tetra-tert-butylcarbazole >98.0%(N) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 1,3,6,8-TETRAKIS(TERT-BUTYL)CARBAZOLE

There total 6 articles about 1,3,6,8-TETRAKIS(TERT-BUTYL)CARBAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

9H-carbazole (86-74-8,105184-46-1,97960-57-1) + tert-butyl alcohol (75-65-0) → 1,3,6,8-tetra-tert-butyl-9H-carbazole (34601-54-2)

Guidance literature:

With trifluoroacetic acid; Heating;

DOI:10.1007/BF00499409

Reference yield: 92.0%

tertiary butyl chloride (507-20-0) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 1,3,6,8-tetra-tert-butyl-9H-carbazole (34601-54-2)

Guidance literature:

With aluminium trichloride;

Reference yield: 30.0%

tertiary butyl chloride (507-20-0) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 1,3,6,8-tetra-tert-butyl-9H-carbazole (34601-54-2) + 1,3,6-tri(tert-butyl)carbazole (34601-53-1) + 3,6-di(tert-butyl)-9H-carbazole (37500-95-1)

Guidance literature:

With hydrogenchloride; aluminium trichloride; at 20 ℃; for 24h;

DOI:10.1021/jo801132w

upstream raw materials:

tertiary butyl chloride

9H-carbazole

isobutene

tert-butyl alcohol

Downstream raw materials:

3,6-di(tert-butyl)-9H-carbazole

Refernces

• 1、 -. "RECHARGEABLE LITHIUM-ION CELL". Paragraph 0068. . Retrieved 2017/06/30.
• 2、 Kuhn, Norbert,Schulten, Michael,Boese, Roland,Blaeser, Dieter. "Synthesis and Structure of 1,3,6,8-Tetra-tert-butylcarbazole". . p. 1503 - 1508. Retrieved 2007/10/02.