N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

Base Information

Chemical Name:N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide
CAS No.:958332-57-5
Molecular Formula:C₁₄H₂₃ClN₂O₃S₂
Molecular Weight:366.933
Hs Code.:

Synonyms:N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

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Chemical Property of N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

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Technology Process of N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

There total 3 articles about N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₂₁ClN₂O₃S₂

: 958332-57-5
N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

Guidance literature:: C₁₄H₂₁ClN₂O₃S₂; With sodium tetrahydroborate; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere; Reflux;

With ethanol; water; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: 95-79-4
5-chloro-2-methyl-benzenamine

: 958332-57-5
N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 20 h / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 24 h / 0 - 20 °C

3.1: titanium(IV) tetraethanolate / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

4.1: sodium tetrahydroborate / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere; Reflux

4.2: 1 h / 20 °C / Inert atmosphere

With pyridine; aluminum (III) chloride; titanium(IV) tetraethanolate; sodium tetrahydroborate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 958332-53-1
N-(4-ACETYL-5-CHLORO-2-METHYLPHENYL)METHANESULFONAMIDE

: 958332-57-5
N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

2.1: sodium tetrahydroborate / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere; Reflux

2.2: 1 h / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; sodium tetrahydroborate; In tetrahydrofuran;