N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE

Base Information

Chemical Name:N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE
CAS No.:958332-58-6
Molecular Formula:C₁₀H₁₅ClN₂O₂S*ClH
Molecular Weight:299.221
Hs Code.:

Synonyms:N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE

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Chemical Property of N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE

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Technology Process of N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE

There total 3 articles about N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 958332-57-5
N-[4-((1R)-1-{[(R)-tert-butylsulfinyl]amino}ethyl)-5-chloro-2-methyl-phenyl]methanesulfonamide

: 958332-58-6
N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE

Guidance literature:: With hydrogenchloride; In methanol;

Reference yield:

: 95-79-4
5-chloro-2-methyl-benzenamine

: 958332-58-6
N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 20 h / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 24 h / 0 - 20 °C

3.1: titanium(IV) tetraethanolate / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

4.1: sodium tetrahydroborate / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere; Reflux

4.2: 1 h / 20 °C / Inert atmosphere

5.1: hydrogenchloride / methanol

With pyridine; hydrogenchloride; aluminum (III) chloride; titanium(IV) tetraethanolate; sodium tetrahydroborate; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: C₁₄H₂₁ClN₂O₃S₂

: 958332-58-6
N-{4-[(1R)-1-AMINOETHYL]-5-CHLORO-2-METHYLPHENYL}METHANESULFONAMIDE HYDROCHLORIDE

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere; Reflux

1.2: 1 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride / methanol

With hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran; methanol;