2-(But-1-en-2-yl)aniline

Base Information

Chemical Name:2-(But-1-en-2-yl)aniline
CAS No.:246019-65-8
Molecular Formula:C₁₀H₁₃N
Molecular Weight:147.22
Hs Code.:
DSSTox Substance ID:DTXSID00441974
Wikidata:Q82258999
Mol file:246019-65-8.mol

Synonyms:246019-65-8;2-(But-1-en-2-yl)aniline;2-(1-Buten-2-yl)aniline;SCHEMBL24385024;DTXSID00441974;AKOS006352419

Suppliers and Price of 2-(But-1-en-2-yl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-(But-1-en-2-yl)aniline

Chemical Property:

PSA：26.02000
LogP:3.27320
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:147.104799419
Heavy Atom Count:11
Complexity:140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(=C)C1=CC=CC=C1N

Technology Process of 2-(But-1-en-2-yl)aniline

There total 6 articles about 2-(But-1-en-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1196-28-7
2'-Aminopropiophenon

: 1779-49-3
Methyltriphenylphosphonium bromide

: 246019-65-8
2-(but-1-en-2-yl)aniline

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

2'-Aminopropiophenon; In tetrahydrofuran; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201606026

Reference yield:

: 1885-29-6
anthranilic acid nitrile

: 246019-65-8
2-(but-1-en-2-yl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 12 h / 0 - 20 °C / Schlenk technique; Sealed tube; Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere; Schlenk technique; Sealed tube

2.2: 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique; Sealed tube

With potassium tert-butylate; In tetrahydrofuran; 2.2: |Wittig Olefination;
DOI:10.1039/c5ob01196e

Reference yield:

: 1196-28-7
2'-Aminopropiophenon

: 2065-66-9
methyl-triphenylphosphonium iodide

: 246019-65-8
2-(but-1-en-2-yl)aniline

Guidance literature:: methyl-triphenylphosphonium iodide; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

2'-Aminopropiophenon; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01615