2,3-diisopropoxybenzaldehyde

Base Information

• Chemical Name: 2,3-diisopropoxybenzaldehyde
• CAS No.: 110654-91-6
• Molecular Formula: C₁₃H₁₈O₃
• Molecular Weight: 222.284
• Mol file: 110654-91-6.mol

Synonyms:2,3-diisopropoxybenzaldehyde

Chemical Property of 2,3-diisopropoxybenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,3-diisopropoxybenzaldehyde

There total 3 articles about 2,3-diisopropoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,3-dihydroxybenzaldehyde (24677-78-9) + isopropyl bromide (75-26-3) → 2,3-diisopropoxybenzaldehyde (110654-91-6)

Guidance literature:

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 50 ℃; for 12h;

DOI:10.1016/S0040-4020(03)01029-9

Reference yield:

3-acetoxy-2-hydroxybenzaldehyde (55477-54-8) + isopropyl bromide (75-26-3) → 3-acetoxy-2-isopropoxy-benzaldehyde (1071611-09-0) + 2,3-diisopropoxybenzaldehyde (110654-91-6)

Guidance literature:

3-acetoxy-2-hydroxybenzaldehyde; With potassium carbonate; In N,N-dimethyl-formamide; for 0.5h; Molecular sieve 4A;

isopropyl bromide; In N,N-dimethyl-formamide; at 50 ℃; for 12h;

Reference yield:

2-iodo-propane (75-30-9) + 2,3-dihydroxybenzaldehyde (24677-78-9) → 2-hydroxy-3-isopropoxybenzaldehyde + 2-isopropoxy-3-hydroxybenzaldehyde (664306-48-3) + 2,3-diisopropoxybenzaldehyde (110654-91-6)

Guidance literature:

2,3-dihydroxybenzaldehyde; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

2-iodo-propane; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

DOI:10.1021/jo901395m

upstream raw materials:

2,3-dihydroxybenzaldehyde

isopropyl bromide

3-acetoxy-2-hydroxybenzaldehyde

2-iodo-propane