tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

Base Information

Chemical Name:tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate
CAS No.:1204430-96-5
Molecular Formula:C₂₇H₄₅NO₃Sn
Molecular Weight:550.369
Hs Code.:

Synonyms:tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

Suppliers and Price of tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

There total 1 articles about tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 99699-32-8
2-methylene-N-phenyl-2-[(tributylstannyl)methyl]propanamide

: 1204430-96-5
tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

Guidance literature:: With (C₂H₅)3N; 4-(dimethylamino)pyridine; In dichloromethane; soln. of Sn compd., Et3N, Boc2O and 4-dimethylaminopyridine in CH2Cl2 stirred at room temp. for 35 h; chromy. (SiO2, hexane/EtOAc 20/1); elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.037

Reference yield: 92.0%

: 64-17-5
ethanol

: 1204430-96-5
tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

: 108286-71-1
ethyl-2-tributylstannylmethyl acrylate

Guidance literature:: With NaH; In ethanol; soln. of Sn compd. in EtOH added to soln. of NaH in EtOH at 0°C, mixt. warmed to room temp., stirred for 1 h, aq. soln. of NH4Cl added; extn. with ethyl acetate, combined org. phases dried over Na2SO4, chromy. (SiO2, hexane/EtOAc 60/1); elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.037

Reference yield: 67.0%

: 67-56-1
methanol

: 1204430-96-5
tert-butyl phenyl(2-[(tributylstannyl)methyl]acryloyl)carbamate

: 132841-83-9
2-(carbomethoxy)allyl tributyltin

Guidance literature:: With NaH; In methanol; soln. of Sn compd. in MeOH added to soln. of NaH in MeOH at 0°C, mixt. warmed to room temp., stirred for 1 h, aq. soln. of NH4Cl added; extn. with ethyl acetate, combined org. phases dried over Na2SO4, chromy. (SiO2, hexane/EtOAc 60/1); elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.037