diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid

Base Information

Chemical Name:diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid
CAS No.:19672-25-4
Molecular Formula:C₁₈H₂₀N₂O₄
Molecular Weight:328.368
Hs Code.:

Synonyms:diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid

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Chemical Property of diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid

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Technology Process of diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid

There total 15 articles about diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 73183-34-3
bis(pinacol)diborane

: 7250-68-2
4,4'-bis(ethoxycarbonyl)azobenzene

: 19672-25-4
diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid

Guidance literature:: bis(pinacol)diborane; 4,4'-bis(ethoxycarbonyl)azobenzene; With pyridine-4-carbonitrile; In pentane; at 70 ℃; for 24h; Inert atmosphere;

With water; In pentane; at 20 ℃; for 0.25h;

Reference yield: 90.0%

: 7250-68-2,122045-06-1
(E)-diethyl 4,4′-(diazene-1,2-diyl)dibenzoate

: 19672-25-4
diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid

Guidance literature:: With methanol; cesium fluoride; bis(pinacol)diborane; at 20 ℃; for 12h; Irradiation;
DOI:10.1021/acs.joc.1c00394

Reference yield: 73.0%

: 99-77-4
ethyl 4-nitrobenzoate

: 94-09-7
p-aminoethylbenzoate

: 19672-25-4
diethyl ester of hydroazobenzene-4,4'-dicarboxylic acid

Guidance literature:: With ammonia; lithium perchlorate; In acetonitrile; at 20 ℃; for 12h; chemoselective reaction; Electrolysis;
DOI:10.1039/d1ob00077b