3-Methyl-1-octylimidazolium tetrafluoroborate

Base Information

• Chemical Name: 3-Methyl-1-octylimidazolium tetrafluoroborate
• CAS No.: 244193-52-0
• Molecular Formula: C12H23BF4N2
• Molecular Weight: 282.133
• Hs Code.: 29339900
• Mol file: 244193-52-0.mol

Synonyms:1-Octyl-3-methyl-imidazolium tetrafluoroborate;

Chemical Property of 3-Methyl-1-octylimidazolium tetrafluoroborate

Chemical Property:

• Melting Point: -88 °C
• Refractive Index: 1.4320 to 1.4360
• PSA: 8.81000
• Density: 1.12 g/cm³
• LogP: 3.97310
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

1-Methyl-3-octylimidazolium tetrafluoroborate ^*data from reagent suppliers

Safty Information:

• Safety Statements: 23-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 3-Methyl-1-octylimidazolium tetrafluoroborate

There total 14 articles about 3-Methyl-1-octylimidazolium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

sodium tetrafluoroborate (13755-29-8) + 1-methyl-3-octylimidazol-3-ium chloride (64697-40-1) → 1-octyl-3-methylimidazolium tetrafluoroborate (244193-52-0)

Guidance literature:

In water; at 20 ℃; for 24h;

DOI:10.1039/d0gc03497e

Reference yield: 95.0%

1-methyl-1H-imidazole (616-47-7) + n-chlorooctane (111-85-3) → 1-octyl-3-methylimidazolium tetrafluoroborate (244193-52-0)

Guidance literature:

With potassium tetrafluoroborate; at 120 - 140 ℃; for 0.5h; microwave irradiation; sonication;

DOI:10.3390/molecules13010149

Reference yield: 94.0%

N-octylimidazole (21252-69-7) + dimethyl sulfate (77-78-1) → 1-octyl-3-methylimidazolium tetrafluoroborate (244193-52-0)

Guidance literature:

N-octylimidazole; dimethyl sulfate; for 0.25h;

With sodium tetrafluoroborate; In water;

upstream raw materials:

1-methyl-3-octylimidazol-3-ium chloride

1-methyl-1H-imidazole

1-bromo-octane

n-chlorooctane

Refernces

• 1、 Pillai, Prathibha,Pal, Nilanjan,Mandal, Ajay. "Synthesis, Characterization, Surface Properties and Micellization Behaviour of Imidazolium-based Ionic Liquids". . p. 1321 - 1335. Retrieved 2017.
• 2、 Schmidt, Fabian,Zehner, Bastian,Kaposi, Marlene,Drees, Markus,Mink, János,Korth, Wolfgang,Jess, Andreas,Cokoja, Mirza. "Activation of hydrogen peroxide by the nitrate anion in micellar media". . p. 1965 - 1971. Retrieved 2021.
• 3、 Hodyna, Diana,Kovalishyn, Vasyl,Rogalsky, Sergiy,Blagodatnyi, Volodymyr,Petko, Kirill,Metelytsia, Larisa. "Antibacterial Activity of Imidazolium-Based Ionic Liquids Investigated by QSAR Modeling and Experimental Studies". . p. 422 - 433. Retrieved 2016.
• 4、 Deng, Aimin,Men, Shuang,Rui, Mu. "Tribromide Ionic Liquids: Probing the Charge Distribution of the Anion by XPS". . p. 1053 - 1056. Retrieved 2020.
• 5、 Adonin, Nikolai Y.,Kazarian, Sergei G.,Martyanov, Oleg N.,Nesterov, Nikolai S.,Prikhod'ko, Sergei A.,Shalygin, Anton S.. "Interactions of CO2 with the homologous series of СnMIMBF4 ionic liquids studied in situ ATR-FTIR spectroscopy: spectral characteristics, thermodynamic parameters and their correlation". . . Retrieved 2020/07/08.