3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

Base Information

Chemical Name:3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide
CAS No.:1207314-89-3
Molecular Formula:C₁₇H₈BrF₁₁N₂O
Molecular Weight:545.15
Hs Code.:

Synonyms:3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

Suppliers and Price of 3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

There total 10 articles about 3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1207314-88-2
N-[2-bromo-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-6-(trifluoromethyl)phenyl]-3-nitro-2-fluorobenzamide

: 1207314-89-3
3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

Guidance literature:: N-[2-bromo-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-6-(trifluoromethyl)phenyl]-3-nitro-2-fluorobenzamide; With hydrogenchloride; tin(ll) chloride; In ethanol; water; at 60 ℃; for 4h;

With sodium hydroxide; In ethanol; water; pH=10;

Reference yield:

: 1207314-87-1
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

: 1207314-89-3
3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium fluoride / N,N-dimethyl-formamide / 10 h / 130 °C / Inert atmosphere

2.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 4 h / 60 °C

2.2: pH 10

With hydrogenchloride; potassium fluoride; tin(ll) chloride; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1207314-85-9
4-(perfluoropropane-2-yl)-2-(trifluoromethyl)aniline

: 1207314-89-3
3-amino-N-[2-bromo-4-[1,1,1,2,3,3,3-heptafluoroprop-2-yl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 60 °C

2.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 1 h / -70 - 20 °C

3.1: potassium fluoride / N,N-dimethyl-formamide / 10 h / 130 °C / Inert atmosphere

4.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 4 h / 60 °C

4.2: pH 10

With hydrogenchloride; potassium fluoride; N-Bromosuccinimide; tin(ll) chloride; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; water; N,N-dimethyl-formamide;