tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

Base Information

Chemical Name:tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate
CAS No.:1445088-24-3
Molecular Formula:C₃₈H₄₁NO₁₇
Molecular Weight:783.74
Hs Code.:

Synonyms:tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

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Chemical Property of tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

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Technology Process of tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

There total 4 articles about tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1445088-14-1
tetraallyl ((3R,4S,5R,6R)-6-(hydroxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

: 701913-55-5
para-nitrophenyl para-(phenylacetamido)benzylcarbonate

: 1445088-24-3
tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

Guidance literature:: With dmap; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1039/c3cc43702g

Reference yield:

: 54325-28-9
6-O-trityl-D-glucopyranose

: 1445088-24-3
tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N,N,N,-tetramethylethylenediamine / dichloromethane / 1 h / 0 °C

2: toluene-4-sulfonic acid / dichloromethane; water; methanol / 6 h / 20 °C

3: dmap / tetrahydrofuran / 24 h / 20 °C

With dmap; N,N,N,N,-tetramethylethylenediamine; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c3cc43702g

Reference yield:

: 1445088-09-4
tetraallyl ((3R,4S,5R,6R)-6-((trityloxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

: 1445088-24-3
tetraallyl (3R,4S,5R,6R)-6-((4'-(2''-phenylacetamido)carboxybenzoxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl) tetracarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / dichloromethane; water; methanol / 6 h / 20 °C

2: dmap / tetrahydrofuran / 24 h / 20 °C

With dmap; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c3cc43702g