2,4-DICHLORO-5-NITRO-PHENYLAMINE

Base Information

• Chemical Name: 2,4-DICHLORO-5-NITRO-PHENYLAMINE
• CAS No.: 34033-44-8
• Molecular Formula: C6H4 Cl2 N2 O2
• Molecular Weight: 207.016
• Hs Code.: 2921420090
• Mol file: 34033-44-8.mol

Synonyms:Aniline,2,4-dichloro-5-nitro- (8CI); 2,4-Dichloro-5-nitroaniline;2,4-Dichloro-5-nitrobenzenamine; 2-Nitro-4-amino-1,5-dichlorobenzene

Chemical Property of 2,4-DICHLORO-5-NITRO-PHENYLAMINE

Chemical Property:

• PSA: 71.84000
• LogP: 3.58820

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,4-DICHLORO-5-NITROANILINE AldrichCPR ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-DICHLORO-5-NITRO-PHENYLAMINE

There total 6 articles about 2,4-DICHLORO-5-NITRO-PHENYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,4-dichloro-1,5-dinitrobenzene (3698-83-7) → 2-nitro-4-amino-1,5-dichlorobenzene (34033-44-8)

Guidance literature:

With hydrogen; iron; acetic acid; palladium dichloride; In ethanol; at 20 - 25 ℃; under 258.6 - 2327.2 Torr;

DOI:10.1016/S0040-4039(00)97008-4

Reference yield: 42.0%

2,4-Dichloroaniline (554-00-7,51908-09-9) → 2-nitro-4-amino-1,5-dichlorobenzene (34033-44-8)

Guidance literature:

With sulfuric acid; nitric acid; at -20 ℃; for 3.25h;

DOI:10.1021/jf200616y

Reference yield:

methanol (67-56-1) + chlorine (7782-50-5) + 3-nitro-aniline (99-09-2) → 4-Chloro-3-nitroaniline (635-22-3) + 2,4,6-trichloro-3-nitro-aniline (62406-71-7) + 2-nitro-4-amino-1,5-dichlorobenzene (34033-44-8)

Guidance literature:

upstream raw materials:

2,4-dichloro-1,5-dinitrobenzene

sulfuric acid

methanol

chlorine

Downstream raw materials:

2-bromo-4,6-dichloro-3-nitroaniline

1-bromo-3,5-dichloro-6-propylthio-2-nitrobenzene

1-bromo-3,5-dichloro-2,6-dinitrobenzene

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