2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline

Base Information

Chemical Name:2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline
CAS No.:1567334-98-8
Molecular Formula:C₂₈H₃₆ClN₃O
Molecular Weight:466.066
Hs Code.:

Synonyms:2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline

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Chemical Property of 2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline

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Technology Process of 2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline

There total 3 articles about 2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1567334-91-1
2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N-ethylaniline

: 75-03-6
ethyl iodide

: 1567334-98-8
2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline

Guidance literature:: With potassium carbonate; In acetone; at 60 ℃;

Reference yield:

: 1567334-90-0
5-(4-chlorophenyl)-1-(2-nitrophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazole

: 1567334-98-8
2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; iron / ethanol / 1 h / 90 °C

2.1: tetrahydrofuran / 0.25 h

2.2: 72 h

3.1: potassium carbonate / acetone / 60 °C

With iron; potassium carbonate; acetic acid; In tetrahydrofuran; ethanol; acetone;

Reference yield:

: 1567334-93-3
2-(5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl)aniline

: 1567334-98-8
2-[5-(4-chlorophenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazol-1-yl]-N,N-diethylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 0.25 h

1.2: 72 h

2.1: potassium carbonate / acetone / 60 °C

With potassium carbonate; In tetrahydrofuran; acetone;