1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol

Base Information

Chemical Name:1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol
CAS No.:219932-11-3
Molecular Formula:C₃₀H₃₄O₇
Molecular Weight:506.596
Hs Code.:

Synonyms:1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol

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Chemical Property of 1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol

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Technology Process of 1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol

There total 5 articles about 1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 824-94-2
p-methoxybenzyl chloride

: 13265-84-4
D-glucal

: 219932-11-3
1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 60 ℃; for 5.5h;
DOI:10.1039/b303817c

Reference yield: 72.0%

: 824-94-2
p-methoxybenzyl chloride

: 2873-29-2
D-glucal triacetate

: 219932-11-3
1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol

Guidance literature:: D-glucal triacetate; With sodium methylate; In methanol; at 0 - 20 ℃; for 1h;

p-methoxybenzyl chloride; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 5h;
DOI:10.1021/acs.joc.1c01318

Reference yield: 64.0%

: 67-56-1
methanol

: 3,4,6-tri-O-(p-chlorobenzyl)-D-glucal

: 219932-11-3
1,5-anhydro-2-deoxy-3,4,6-tri-O-(4-methoxybenzyl)-D-arabino-hex-1-enitol

Guidance literature:: With di-tert-butyl (2’,4’,6’-triisopropyl-3,6-dimethoxy-[1,1‘-biphenyl]-2-yl)phosphine; methanesulfonato(2-(di-tert-butylphosphino)-3-methoxy-6-methyl-2′,4′,6′-tri-isopropyl-1,1′-biphenyl)(2′-amino-1,1′-biphenyl-2-yl)palladium(II); caesium carbonate; In 1,4-dioxane; at 60 ℃; for 5.5h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02672